Calibration is a vital and
mandatory process in the utilization of measuring instruments by any business
unit. The reliability of the test results generated by an instrument is
established by the calibration report of that instrument. Any laboratory
involved in third party testing or Quality control of a process industry should
take its calibration activities seriously.
Before presenting an exposition
on the topic or subject of Calibration, it will be useful to understand the
need for calibrating instruments. First of all, let us make one thing clear
that we need to calibrate measuring instruments only and not those instruments
or machines which do not generate any data for measurement purposes. Now, the
importance of calibration stems from the fact that, in order to establish
reliability in the test results we need to have some kind of verification
process in place. This purpose is solved by reliable calibration services.
Accuracy in a calibration process ensures accuracy in the data obtained from an
analytical measuring instrument.
Before we can embark upon
exploring all the details and intricacies of ‘Calibration’, we need to define
it. There are a number of standard definitions of Calibration specified by
various standard bodies, but simply put Calibration can be defined as the
process or set of operations needed for comparing the results produced by the
instrument being calibrated, with that of standards being used for calibration.
These standard substances are also known as Standard Reference Materials or
Calibrators, and these must be already calibrated against far more
accurate reference standards which are traceable to SI units. Sometimes,
calibration can also mean to configure or manipulate instruments to give values
as determined by those of standards. The choice of reference standards depends
on the type of instrument being calibrated, i.e. specifications (like least
count), and also on the accuracy requirements of the measurement process. Types
of instruments requiring calibration can range from relatively small ones like
weighing balances, pressure gauges, ovens to large ones that are used in
industries like automobiles etc. The type of calibrators also varies with the
kind of instrument requiring calibration.
The time required for calibration
varies with the type of instrument being calibrated, and also on the purpose of
calibration. As a rule of thumb, the time period for a particular calibration
is directly proportional to the degree of accuracy demanded. Hence, a very
sensitive instrument will require longer time to get calibrated as compared to
a less sensitive one. Another aspect concerning calibration is the frequency of
calibration. This depends, among a number of factors, on (1) manufacturer’s recommendations,
(2) tendency to wear & drift, (3) frequency and severity of use, (4)
environmental conditions (like lab climate, vibrational levels, etc.) & (5)
recorded history of maintenance and servicing.
Like no measurement result can be
free of error and a certain degree of uncertainty is associated with it,
similarly calibration reports also state the value of uncertainty involved
in the process of calibration for a particular instrument. So, every test
result produced by a measuring instrument has a limit of certainty defined by
the uncertainty value. Calibration services are required for a number
of different fields like mechanical, thermal, electro-technical, analytical
etc. Ensuring calibration of instruments is the key to maintaining faith
amongst customers and carrying out business in a smooth manner.
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